
Laboratory
Equipment - June 2007
Laboratory Design & Furnishings
Improving AFM Data Reliability in Nanoelectronics
Research
Negative-Stiffness
Vibration Isolation Eliminates Ultra-Low Environmental Frequencies
and Improves Data Set Integrity
By Jim McMahon
It was long after
1977 that the name "nanoelectronics" came into use,
though Dr. David K. Ferry was already actively engaged in
developing some of the world's smallest transistors. The field,
which at the time was called "Ultra-Small Devices",
was in its infancy and Dr. Ferry's research team was one of
only four select groups researching the limits of small electronic
devices.
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Today,
Dr. Ferry heads up the Nanostructures Research Group
at Arizona State University (ASU) in Tempe, a collection
of faculty, staff and students working on research in
the regimes of nanolithography, the physics of nanostructures
and ultra-small semiconductor devices. The group is
part of the University's College of Engineering, Center
for Solid State Electronics Research, whose alumni make
up a serious constituency throughout the nanoelectronics
universe in both industry and academia.
Their current interests lie in the area of quantum dots,
quantum wires and ultra-small semiconductor devices
in a variety of materials. The group conducts a wide
array of theoretical studies of quantum transport in
these very small devices. For example, they are involved
in a process called scanning gate microscopy at low
temperatures. This involves taking the equivalent of
an atomic force microscope, putting bias on it, and
studying the change in conductance of small semiconductor
structures as they move this bias tip around on a surface.
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ASUs
Dewar sitting on Negative-Stiffness vibration isolation
tables.
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The system is mounted
in a large cryogenic cooler, an enclosed container with a helium-3
cooling system, an isotope of a helium molecule-which is brought
down to 300 milli-Kelvin, or 1000 times below room temperature,
about one-half a degree above absolute zero. The cooler has
a vacuum jacket around it so the heat can't transmit in, and
it prevents the cold from being mitigated by the ambient room
temperature.The AFM tip is on a cantilever. Normally, with the
AFM, one moves the cantilever along the surface and then notes
the change in position as it goes over topography on the surface.
Dr. Ferry's group is utilizing a process called a piezo-electric
sensor in which they metalicize the AFM cantilevered tip with
a very thin layer of metal so they can apply a voltage to it.
They then use that voltage to perturb the structure they are
looking at. As the tip moves it creates a voltage across the
plane, which is measured to determine certain mechanical property
values. This is a technique that was developed four or five
years ago at Harvard University.
High Level of Vibration Isolation Required
When measuring a very few angstroms or nanometers of displacement,
an absolutely stable surface upon which to rest your instrument
is critical. If not, any of the vibration coupled into the mechanical
structure of the instrument will cause vertical noise and fundamentally
an inability to measure these kinds of high resolution features.

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"Any kind of vibration noise in the system makes
the AFM cantilever tip move, and that gives you bad
signals and incorrect data," says Dr. Ferry. "We
actually went further than most university applications
because we integrated a rather large magnet into our
system, something that Harvard, for example, is just
now putting into their operation. The magnet allows
us to look at different types of transport. We can turn
the magnet on and look at the magneto-transport of the
semiconductors. It is a quite a different mode of transport
altogether."
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Top
portion of the Dewar.
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"The entire system had to be isolated, not just the cantilever,"
continues Dr. Ferry. "We required an extremely high level
of vibration isolation given our research parameters. We are
deriving modern electronic devices from our experiments. Future
electronic devices are our interest. What we are doing is looking
at the conductivity of materials and then seeing how quantum
mechanics fits into this. We study basic physics, which has
a real application-engineering-particularly in the semiconductor
industry."
Dr. Ferry's Research
Covers:
(1) Electron beam lithography of quantum dots and quantum
devices, with applications such as quantum ballistic transport
at very low temperatures and high magnetic fields, as well as
the quantum-classical transition and the role of quantum effects
in real devices at room temperature.
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Viewgraph showing images in GaAs
where the random potential is absent.
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(2)
Magneto-transport studies used to probe the nature of
electron dynamics in semiconductor quantum dots, which are
quasi-zero-dimensional structures whose size is comparable
to the Fermi wavelength of the electrons themselves. Magneto-transport
studies may be used to probe these phenomena and to determine
the factors which limit electron phase coherence within the
structures. Current interest in these devices is motivated
by their potential application in new areas of technology,
such as quantum computing and ultra high frequency signal
processing.
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Surface chemical analysis performed with a scanning
Auger microprobe. Under good conditions, a lateral resolution
of about 25 nm is achievable.
(4) Professor Michael Kozicki, in the group, has examined
Chemically Enhanced Vapor Etching (CEVE) patterning
technique. He has used hydrocarbon contamination
layers from laboratory air or vacuum chamber ambients
and successfully demonstrated nanoscale pattern formation
in silicon dioxide.
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AFM image of a quantum point contact showing isolation
benches
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He has also developed a nitrogen chamber coupled directly
to a UHV STM/AFM facility for CEVE processing of silicon
dioxide resists, and their use in semiconductor device fabrication.
Within the nitrogen chamber there is a processing system
for the actual CEVE development.
Scanning gate image of the random potential in
presence of a magnetic field
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"But,
the current work with the scanning probe system
is really interesting, and made possible by the
negative-stiffness isolators," Dr. Ferry concludes.
The negative-stiffness isolator, a passive isolation
approach, has a key advantage in that it is not
powered -- it has no electricity going to it. So,
in a site where heat buildup could be an issue,
such as with enclosed cryogenic chambers, negative-stiffness
becomes a highly efficient option.
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AFM image of quantum interference rings which occur
in the interior regions of a quantum dot
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Negative-stiffness
isolators employ a mechanical concept in low-frequency
vibration isolation. Vertical-motion isolation is
provided by a stiff spring that supports a weight
load, combined with a negative-stiffness mechanism
(NSM). The net vertical stiffness is made very low
without affecting the static load-supporting capability
of the spring. Beam-columns connected in series
with the vertical-motion isolator provide horizontal-motion
isolation. The horizontal stiffness of the beam-columns
is reduced by the "beam-column" effect.
(A beam-column behaves as a spring combined with
an NSM.) The result is a compact passive isolator
capable of very low vertical and horizontal natural
frequencies and very high internal structural frequencies.
The isolators (adjusted to 1/2 Hz) achieve 93% isolation
efficiency at 2 Hz, 99% at 5 Hz, and 99.7% at 10
Hz.
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isolators provide a capability quite unique to the field
of nanotechnology -- specifically, the transmissibility
of the negative-stiffness isolator, that is, the vibration
that transmits through the isolator as measured as a
function of floor vibrations -- which is substantially
improved over active isolation systems. Although active
isolation systems fundamentally have no resonance, their
transmissibility does not roll off as fast as negative-stiffness
isolators. So, at building and seismic frequencies the
transmissibility of active isolators can be 10X greater
than negative-stiffness isolators. This causes substantial
adverse measurement and imaging artifacts in the data.
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Negative stiffness isolation performance by transmissibility.
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Compared to other laboratory research instrumentation, the
growth of AFM usage has been quite extensive over the past
10 years. AFM equipment placement has gone through a doubling
phase pretty much every year during the last decade. Since
its inception in 1988, it has continuously proven to be a
key tool in moving nanotechnology research forward.
"More
than half of the universities in the United States, and worldwide,
are engaging in nanotechnology research," says Dr. Ferry.
"In the electronic area, the nanoelectronic side of it
has been going since the late 1960s. This is driven by the
fact that in the semiconductor industry all things are getting
smaller and smaller.
Today, the
transistors have critical dimensions down around 25 nanometers.
And the most critical dimension is the oxide thickness, which
is 1 nanometer. When you consider that you have to control
one nanometer vertical thickness over 300 millimeters of lateral
dimension, that is a difference of 10 to the 8th power. That
defines what modern manufacturing technology produces. The
need for effective vibration isolation has never been greater,
and will continue to become more demanding as the nano-industry
progresses."
David
K. Ferry, Ph.D., M.S.E.E., B.S.E.E.,
is a Regents' Professor of Electrical Engineering; recipient
of the Arizona State University Graduate Mentor Award, 2001;
and recipient of the IEEE Cledo Brunetti Award, 1999 for fundamental
contributions to the theory and development of nanostructured
devices.
For more information
contact Steve Varma at Minus K Technology, Inc at sales@minuk.com
or by phone at 310-348-9656.
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